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The first configuration is useful to evaluate the electrochemical behavior of pure microelectrode arrays for correlating it with model equations. The second configuration is particularly useful when the substrate material by itself is inactive for the studied reaction. These arrays were employed for studying the hydrogen oxidation reaction in alkaline medium on Au/Rh and on GC/Rh in order to detect possible kinetic interactions of both components at the heterojunctions. Quimica aplicada a la medicina. In the latter case, any detected differences between the electrochemical behavior of the PMMA‐coated array and that of the bi‐component array should come from the contributions of the microelectrode boundaries.

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